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장비명
DiffusIR
측정방식
Diffuse reflection
측정샘플
난반사가 일어나는 고체 샘플, 분말
특 징
열역학, 반응 매커니즘, 촉매 연구
크기/무게
W 180 x D 230 x H 130 mm
적용장비
FTIR

DiffusIR

 

.  가열, 냉각, 고진공 및 고압 애플리케이션을 위한 환경 챔버(옵션)를 수용할 수 있는 연구용 악세사리

.  이 특수 챔버는 물질의 열역학적 특성을 연구하고, 반응 매커니즘을 결정하고, 촉매 연구를 수행하는 데 사용할 수 있음

.  Optical design: 3X ellipsoidal

.  입사각: 30도

.  Sample focus: Micrometer

.  Sample positions: 2 positions, slide stops for background and sample with no purge loss

.  Sample cups: Micro: 6 x 1.6mm deep / Macro: 10 x 2.3mm deep

 

Environmental Chamber Specifications

.  Temperature range, HTV: Ambient to 500 or 1000°C

.  Temperature range, LTV: -150 to 500°C

.  Heating rate, Maximum: Up to 120°C /minute, 500/ 1000°C

.  Temperature control: Digital

.  Window size: 32 x 3mm disk (vacuum) / 32mm ZnSe dome (pressure)

.  Leak Rate: < 6.0 x 10-11 Pa m3/sec

.  Pressure maximum: 1500 psi, with High-pressure adaptor (available in HTV versions only) / 14.7 psi (1 atmosphere) using KBr window

.  Sample cup size: Macro: 6.0mm OD, 4.0mm height / Micro: 4.7 mm ID, 2.0mm depth

 

기본구성

.  10041-10XX DiffusIR Accessory includes sample preparation kit with 2 micro and 2 macro sample cups, sample loading tools, abrasion sampling kit, SiC and diamond sampling disks, alignment mirror, 35mm mortar with pestle and KBr powder

.  10041-60XX DiffusIR Accessory with Gold-Coated optics includes sample preparation kit with 2 micro and 2 macro sample cups. sample loading tools, abrasion sampling kit, SiC and diamond sampling disks, alignment mirror, 35mm mortar with pestle and KBr powder

.  Temperature controller 등 선택 가능

 

선택구성

.  DiffusIR Options

 

 

 Part Number

  Desciption

 10162-4150

  DiffusIR Environmental Chamber, HTV, ambient to 500°C

 10162-4200

  DiffusIR Environmental Chamber, HTV, ambient to 1000°C

 10162-4180  

  High-Pressure Adapter Dome for Chambers, HTV

 10162-4140

  DiffusIR Environmental Chamber, LTV, -150 to 500°C

 

.  Temperature Control Modules

 

 Part Number

  Description

 10076-2550

  Digital Temperature Control Module

 10007-0207

  PIKE TempPRO Software

 10162-4165

  Liquid Nitrogen-Cooled System and Temperature Control Module DiffusIR Environmental Chamber, LTV, -150 to 500°C

 

.  Replacement Parts and Supplies

 

 Part Number

  Description

 10170-1100

  Liquid Recirculator

 10042-2010

  Sample cup, micro, 6mm diameter, 1.6mm deep

 10042-2020

  Sample cup, macro, 10mm diameter, 2.3mm deep

 10042-3030

  Sample cup holder and base

 10160-8010

  KBr powder

 10042-3040

  Sample preparation kit

 10042-3010

  Abraison sampling kit

 10042-3020

  Abraison disks, silicon carbide

 10042-3025

  Abraison disks, diamond

 10042-3060

  Flat sample post

 10042-3080

  Alignment mirror, aluminum

 10042-3082

  Alignment mirror, gold

 10162-4298

  Rotary pump for vacuum insulation, 115V

 10162-4299

  Rotary pump for vacuum insulation, 230V

 

.  Replacement parts and supplies

 

 Part Number

  Description

 10160-1132

  Disk, KBr, 32 x 3mm

 10160-1113

  Disk, ZnSe, 32 x 3mm

 10160-1231

  Disk, ZnSe, 32 x 3mm, with anti-reflective coating

 10160-5049

  Disk, SiO2, 32 x 3mm

 10160-5125

  Disk, SiO2, 32 x 3mm, low OH

 10160-1159

  Disk, Si, 32 x 3mm

 10162-4210

  O-Ring for DiffusIR chamber

 10162-4215

  O-Ring for DiffusIR chamber cooling line

 10162-4251

  Ceramic cup for DiffusIR chamber, porous

 10162-4270

  Alignment mirror for DiffusIR chamber